Stability of high-mass molecular libraries

Author(s)
Ugur Sezer, Philipp Schmid, Lukas Felix, Marcel Mayor, Markus Arndt
Abstract

Molecular beam techniques are a key to many experiments in physical chemistry and quantum optics. In particular, advanced matter-wave experiments with high-mass molecules profit from the availability of slow, neutral and mass-selected molecular beams that are sufficiently stable to remain intact during laser heating and photoionization mass spectrometry. We present experiments on the photostability with molecular libraries of tailored oligoporphyrins with masses up to 25 000 Da. We compare two fluoroalkylsulfanyl-functionalized libraries based on two different molecular cores that offer the same number of anchor points for functionalization but differ in their geometry and electronic properties. A pentaporphyrin core stabilizes a library of chemically well-defined molecules with more than 1600 atoms. They can be neutrally desorbed with velocities as low as 20 m/s and efficiently analyzed in photoionization mass spectrometry.

Organisation(s)
Quantum Optics, Quantum Nanophysics and Quantum Information
External organisation(s)
Universität Basel, Karlsruher Institut für Technologie
Journal
Journal of Mass Spectrometry
Volume
50
Pages
235-239
No. of pages
5
ISSN
1076-5174
DOI
https://doi.org/10.1002/jms.3526
Publication date
01-2015
Peer reviewed
Yes
Austrian Fields of Science 2012
104015 Organic chemistry, 103026 Quantum optics, 104017 Physical chemistry, 103006 Chemical physics
Keywords
ASJC Scopus subject areas
Spectroscopy
Portal url
https://ucrisportal.univie.ac.at/en/publications/80292548-f804-47b6-a84e-54a856d410ed